网络讲座 | Integrated Differential Phase Contrast (iDPC)-STEM

2021-10-25 19:02:24, 赛默飞 赛默飞材料表征仪器


01

主讲人简介

Dr. Ivan Lazić

Dr. Ivan Lazić is currently a science, technical and project lead at Thermo Fischer Scientific, Department of Materials & Structural Analysis in Eindhoven, The Netherlands. Since 2011 he holds a position of a senior scientist working on fundamental understanding of the contrast formation and detection in (Scanning) Transmission Electron Microscopy (S)TEM. The main focus is on improvement of the existing imaging and detection techniques as well as on investigating and suggesting novel ones. He is main inventor and developer of the iDPC-STEM, coinventor and developer of Segmented Ptychography, and a contributor to other (S)TEM related innovations. In parallel, he focuses on developing theoretical and analytical description of (S)TEM imaging.

He presented his work on various occasions as invited speaker in Europe, including UK (Oxford), US (including Princeton), Japan, South Korea, India, Australia and China. He is an author of many journal papers, patents and a book chapter on STEM.

Prior to this, he accomplished a post-doctorate at Delft University of Technology (TU Delft), The Netherlands, Faculty of Applied Sciences and Kavli Institute of Nanoscience, working on ultimate resolution of electron and ion beam induced deposition and lithography (EBID, IBID and EBL).

Dr. Lazić obtained his PhD degree in 2009 from TU Delft, The Netherlands, Department of Material Science and Engineering (Thesis: Atomic scale simulations of oxide and metal film growth). Previously he graduated and received his master degree in 2003 at University of Belgrade, Serbia, Faculty of Electrical Engineering, Department of Physical Electronics, Optoelectronics and Laser engineering (Thesis: Electron transport and photon emission in Si/Ge hetero-structures of quantum cascade lasers). As an undergraduate he carried out an internship at Swiss Federal Institute of Technology, ETH, Zürich, Switzerland, Department of Physical Electronics.

02

内容简介

A state-of-the-art STEM phase imaging technique called Integrated Differential Phase Contrast STEM (iDPC-STEM) [1, 2] will be presented, both from fundamental and theoretical point of view up to practical implementation and applications. Beside regular conditions, iDPC-STEM ability will be demonstrated also at the limit of resolution, contrast, and dose [3] for wide variety of samples.

First, it will be shown that iDPC-STEM is an elegant solution to the well-known phase problem in TEM, with the full capacity to resolve the atoms at sub-Å scale from 30 keV to 300 keV under various (including extreme) conditions.

Second, its ability to image both light and heavy elements together [2, 3, 4], long range fields (such as strain and build in contact potentials), metallization and thickness variations, both for amorphous and crystalline materials, thin as well as thick samples [5] will be demonstrated. For the reference, simultaneous results with ADF-STEM will be presented in most of the cases.

Finally, examples will be shown of clear and unambiguous iDPC-STEM imaging of extremely light elements, including hydrogen [6], single molecule imaging [7], as well as low dose imaging of beam sensitive materials. Images of Zeolites (ZSM-5) [2, 8] and Metal Organic Frameworks (MOFs) using dose of only 120 e-/Å2 while demonstrating resolution of 1.6 Å will be presented (MIL-53 (Al) [100]), as well as 45 e-/Å2 while demonstrating resolution of 2.0 Å (MIL-101). For completeness a cryo-STEM imaging, single particle analysis (SPA) acquisition and reconstruction of Tobacco Mosaic Virus (TMV) will be shown at near atomic resolution [9].

References:

[1]I. Lazić, E.G.T. Bosch and S. Lazar, Ultramicroscopy 160 (2016) 265-280.

[2]I. Lazić, E.G.T. Bosch, Advances in Imaging and Electron Physics 199 (2017) 75-184.

[3]E. Yücelen, I. Lazić, E.G.T. Bosch, Scientific Reports 8 (2018) pp-pp.

[4]D. Song, et.al., Advanced Functional Materials (2019) 1903843.

[5]E.G.T. Bosch, I. Lazić, Ultramicroscopy 207 (2019) 112831.

[6]S. de Graaf et.al., Science Advanced 6, eaay4312.

[7]B. Shen, et. al., Nature 592, 541–544 (2021).

[8]I. Lazić, et. al. Microsc. Microanal 22, 36-37 (2016).

[9]I. Lazić, et. al. bioRxiv, doi: https://doi.org/10.1101/2021.10.12.464113 (2021).



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  • 客服电话: 400-6699-117 转 1000
  • 京ICP备07018254号
  • 电信与信息服务业务经营许可证:京ICP证110310号
  • 京公网安备1101085018

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